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1.
采用HPTA方法对长江口水中硼进行分析,并与姜黄素法进行比较,方法的标准偏差为0.005,变动系数小于5%,对长江口水样分析结果与姜黄素法相比较,其相对误差为-0.4%。  相似文献   
2.
Over the past two decades, “illegal” natural resource extraction has become a significant driver of environmental change and social conflict across the Global South. In response, numerous Sub-Saharan African states have engaged in governance reforms that heed calls to securitize – or, establish and consolidate state control over – natural resources. In Ghana, securitization has served to entrench the informal economy as domestic producers, marginalized in the process of reform, continue to utilize non-state institutions to maintain access. While the Ghanaian state has branded “illegal” resource extraction a major environmental, social, and national security concern, it has responded to this threat unevenly; it has violently enforced its authority in some contexts but remained relatively indifferent in others. This article explores the phenomenon of selective enforcement to explain patterns of violence that have emerged between state and society in response to both securitization and informality. Drawing on a multimethod approach, I find that natural resource governance authority remains fragmented across resource contexts, and that the configuration of authority and interests on the ground shapes the extent of state intervention. I propose a natural resource typology that identifies when the state is most likely to enforce its authority, and the degree of violent conflict likely to result. Ultimately, I contend that domestic patterns of enforcement are shaped primarily by: 1) competition with local power holders over resource entitlements and 2) global conservation and extraction priorities. While specific to Ghana, this argument can provide important insights into the relationship between informal extraction, state enforcement, and social conflict in other Global South contexts.  相似文献   
3.
A screening method for heavy metals in aqueous extracts of soil is presented which is based on inhibition of the enzymes urease and alcohol dehydrogenase. The method is suitable to detect cupric and mercury ions in concentrations below 0.01 mg/L and several other heavy metal ions in 1000 fold higher concentration. It is shown that the test may be used for screening of mercury ion concentrations exceeding 0.03 mg/L in aqueous solution when copper chelators are added to the test system. The usefulness of the presented tests to detect heavy metals eluted from soil was verified with samples from ore mining waste. The concentration of copper, lead, and zinc eluted from these samples to different amount was determined by atomic absorption spectrometry and was in good agreement with the enzyme inhibition data obtained with these samples.  相似文献   
4.
论述了采用客户/服务器模型设计、实现化学试剂管理数据库的方法和技术。通过网络平台完成院各部门的年度化学试剂申报、统计和管理工作,可以充分发挥校园网的通讯优势。解决了长期存在的化学试剂手工管理所带来的效率低、申报不及时甚至重复申报等问题。  相似文献   
5.
滇黔桂地区卡林型金矿床成因探讨   总被引:19,自引:2,他引:19  
贾大成  胡瑞忠 《矿床地质》2001,20(4):378-384
矿化剂和沉淀富集剂是成矿物质中的重要组成部分,也是人们分析成矿作用和建立成矿模式的基础。在分析滇黔桂地区金矿地质特征和成矿流体的基础上,提出该类矿床的矿质主要来源于被动陆缘沉积建造,促使金活化、迁移的矿化剂主要是盆地热卤素流体和有机质流体,促使金局部沉淀富集的沉淀富集剂则主要是沉积建造内和深源富硫的流体和热液改造的有机质。认为矿质、矿化剂和沉淀富集剂在有利容矿空间的耦合是形成滇黔桂地区卡林型金矿的主要成矿机制,并在此基础上讨论了卡林型金矿的成因和成矿模式。  相似文献   
6.
Partitioning of heavy metals on soil samples from column tests   总被引:3,自引:0,他引:3  
In this study, column tests were used to determine the retention capability of three types of estuarine alluvia collected adjacent to landfill sites in South Wales. Selective sequential extraction (SSE) was used to study the retention mechanisms of heavy metals in the soil columns obtained from leaching experiments. Acid digestion was later used to check the validity of the SSE results. Breakthrough curves show good retention of heavy metal ions (Pb, Cu, and Zn) by all soils, where almost 99% of heavy metals were retained with the Ce/Co values in the order of 10−3. The retention strength of these soils was observed to be constant up to five pore volumes (PV). This corresponds with the pH of the effluents and pore water of soil slices, which also show good buffering capacity against very acidic leachate up to 5PV. The heavy metal extraction profiles from SSE show very similar trends with the retention profiles from the leaching experiments, where heavy metals were retained mainly at the top part where the leachate entered the column. SSE indicates qualitatively that heavy metals precipitated with carbonates and amorphous materials (oxides/hydroxides) are higher than heavy metal retention via exchangeable mechanisms. The mass balance calculation gives range of deviation of 1–16% of the total soil extraction. The distribution of the heavy metals with various soil constituents are ranked in the following order: Carbonates>Amorphous oxides hydroxides>Organic matter>Exchangeable phases.  相似文献   
7.
报道了新显色剂2-(2-苯并噻唑偶氮)-5-二羧甲氨基苯甲酸(BTACB)的合成,研究了在十二烷基硫酸钠(NaLS)存在下Ni~(2+)与BTACB形成蓝紫色配合物的条件,其λ_(max)~(MR)=600nm,ε=2.79×10~4L·mol~(-1)·cm~(-1),Ni在0~0.6μg/ml范围内服从比尔定律,反应具有一定的选择性。方法已用于直接测定铝合金、纯镁及含一定量Co的钢铁中痕量Ni和经萃取分离后测定纯钴中痕量Ni。  相似文献   
8.
在HAc-NaAc形成的中性缓冲溶液体系中,利用碘的催化动力学原理,使N-N-四甲基-4-4-二氨基二苯甲烷与氯胺T的氧化反应,生成蓝色络合物来测定地探样中微量碘的含量。通过实验,最佳试剂加入量为8%的HAc溶液5mL,8%的Na2CO3溶液3mL,0.1%的N-N-四甲基-4-4-二氨基二苯甲烷溶液5mL所组成的溶液体系中,在加入0.1%的氯胺T1mL显色后,其测定结果准确度、精密度高,检出限低,测定化探样中微量碘时该方法可以推广应用。  相似文献   
9.
采用放射性免疫(RIA)和组织学切片技术,系统地研究了虹鳟(Oncorhynchus mykiss)选育群体的血清性类固醇激素周年变化与性腺发育特点的关系,以及血清中性类固醇激素雌二醇(E2)和睾酮(T)在雌雄亲本中的周年变化规律和生理作用。结果表明,虹鳟性腺发育可划分为6期。雌鱼血清中E2在10月(V期性腺)达到峰值,T浓度在11月达到峰值,而进入繁殖期后(11—12月)E2开始下降。雄鱼血清T浓度在11月达到最大值,E2在6月份达到峰值,在11月之后T开始下降。在各月份,雌鱼E2浓度水平远高于雄鱼,而雄鱼T浓度个别月份低于雌鱼。这些研究揭示出,测定血清性类固醇激素浓度水平可用于准确判断鱼类的生殖状态,且可为虹鳟家系选育出早熟亲本群体提供重要技术依据。  相似文献   
10.
The reduction of discards in European fisheries has been identified as a specific objective of the reform of the EU Common Fisheries Policy. To reduce the uncertainty in catch data and the socially unacceptable waste of resources that results from the disposal of catch at sea, a policy to ban discards has been proposed. Discard bans are currently implemented in Alaska, British Columbia, New Zealand, the Faroe Islands, Norway and Iceland. Experience from these countries highlights that a policy of mandatory landings can result in a reduction in discards, but relies upon a high level of surveillance or economic incentives to encourage fishers to land more of their catch. Discard bans will also not result in long term benefits to stocks unless total removals are reduced, through the avoidance of undersized, non-commercial or over quota catch. Experience shows that additional management measures are required to incentivise such a move towards more selective fishing. Success has resulted from the use of area closures and bycatch limits, with potential applications in EU fisheries. However, selective fishing will not be a panacea for the current state of European fisheries; discard bans and accompanying measures must be embedded in a wider management system that constrains fishing mortality to reasonable levels before sustainable exploitation can occur.  相似文献   
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